HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 117772123, compound → HCID 117774665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 117772123 | HCID 117772123 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 117774665 | HCID 117774665 | — |
Reaction Steps
To 500 mg (1.7 mmol) (2R)-2-[(3-nitro-2-pyridyl)oxy]-N-(2,2,2-trifluoroethyl)propanamide 100 mg Raney-Nickel and MeOH are added and the mixture is hydrogenated in a Parr apparatus (RT; 3 bar; over night). The catalyst is filtered off and the solvent is evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09139577B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-56e006f3758f41eaa0f3088cb5be23e0 |
| Source note | uspto-grants-2015_09 |