HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → 3-Fluoro-4-(4-formylphenoxy)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Fluoro-4-(4-formylphenoxy)benzonitrile | HCID 53425670 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 3-Fluoro-4-(4-formylphenoxy)benzamide | HCID 57352536 | 99% |
Reaction Steps
Hydrolysis of the compound of step 1 using hydrogen peroxide and potassium carbonate in DMSO as described previously afford the above compound in 99% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560463B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-1a96db3b8fc34aa89b4f1710ca0067af |
| Source note | uspto-grants-2009_07 |