HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → 2-amino-N-benzyl-N-methylacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | N-Methylbenzylamine | HCID 7669 | — |
| Reactant | N-(tert-butoxycarbonyl)glycine | HCID 78288 | — |
| Reactant | (S)-(-)-2-Aminomethyl-1-ethylpyrrolidine | HCID 643457 | — |
| Product | 2-amino-N-benzyl-N-methylacetamide | HCID 17932699 | — |
Reaction Steps
By using N-(t-butoxycarbonyl)glycine (1.0 g) and N-methylbenzylamine (736 μl) as a starting material, the title compound (740 mg) was obtained in the same manners as those of Reference Example 88, (1) and Reference Example 78, (3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09139609B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-130aeaeaf18b44ed9daae45a630f7221 |
| Source note | uspto-grants-2015_09 |