HuagongsheHuagongshe Chemistry Print Report · For research reference only
Titanium tetrabutoxide → 3-(Ethylbutoxyphosphinyl)propionic acid titanium salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Titanium tetrabutoxide | HCID 21801 | — |
| Reactant | 3-(Ethylbutoxyphosphinyl)propionic acid | HCID 86656680 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 3-(Ethylbutoxyphosphinyl)propionic acid titanium salt | HCID 131733516 | 97.4% |
Reaction Steps
222 g (1 mol) of 3-(ethylbutoxyphosphinyl)propionic acid (produced as in Example 13) and 85 g of titanium tetrabutoxide are refluxed in 500 ml of toluene for 40 hours. The resulting butanol is distilled off from time to time with proportions of toluene. The solution formed is subsequently freed of solvent to leave 227 g of 3-(ethylbutoxyphosphinyl)propionic acid titanium salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09139714B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-8ba86ee21e7d4696843c520808234b5c |
| Source note | uspto-grants-2015_09 |