HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → 5-Bromo-5'-hexyl-2,2'-bithiophene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 5-Hexyl-2,2'-bithiophene | HCID 15363594 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 5-Bromo-5'-hexyl-2,2'-bithiophene | HCID 59752457 | — |
Reaction Steps
Under a light shielded condition, a 5-hexyl-2,2′-bithiophene (0.66 g, 2.63 mmol)/DMF (10 mL) solution was added to NBS (0.56 g, 3.16 mmol) and reacted for one hour. The reaction mixture was then washed with water and was extracted with diethyl ether. The organic layer was dried with MgSO4, and then the solvent was removed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09139774B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-e23eb2998d094ab9ac21b0e5dd04d261 |
| Source note | uspto-grants-2015_09 |