反应详情

Under a light shielded condition, a 5-hexyl-2,2′-bithiophene (0.66 g, 2.63 mmol)/DMF (10 mL) solution was added to NBS (0.56 g, 3.16 mmol) and reacted for one hour. The reaction mixture was then washed with water and was extracted with diethyl ether. The organic layer was dried with MgSO4, and then the solvent was removed.

1. customreacted for one hour
2. washThe reaction mixture was then washed with water
3. extractionwas extracted with diethyl ether
4. dry with materialThe organic layer was dried with MgSO4
5. customthe solvent was removed