HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58095051, compound → HCID 58095099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58095051 | HCID 58095051 | — |
| Reactant | HCID 58095108 | HCID 58095108 | — |
| Product | HCID 58095099 | HCID 58095099 | — |
Reaction Steps
The title compound was prepared from 1-allyl-2-[3-(2,4-dichlorophenyl)-5-(tributylstannyl)-2-thienyl]-1H-imidazole and 7-iodo[1,3]oxazolo[4,5-b]pyridin-2(3H)-one using procedures analogous to those described in Example 8-A, Steps 2 and 3. LC/MS (AA) ES+ 429, 431. 1H NMR (400 MHz, d6 DMSO) δ: 8.03 (d, J=5.77 Hz, 1H), 7.83 (s, 1H), 7.59 (d, J=2.01 Hz, 1H), 7.43-7.39 (m, 2H), 7.36 (d, J=8.29 Hz, 1H), 7.06 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09139589B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-a69dd11c00d749f59dc2d9bfdf170d4f |
| Source note | uspto-grants-2015_09 |