HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Bromo-3-methylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Bromo-3-methylbenzoic acid | HCID 82131 | — |
| Product | 4-Bromo-3-methylbenzoyl chloride | HCID 7021534 | — |
Reaction Steps
A mixture of 4-bromo-3-methylbenzoic acid (5.0 g, 23.25 mmol) and thionylchloride (50 ml) was refluxed for 5 hours. After removal of thionyl chloride, the residue was dried under high vacuum and used in next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09139868B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-7cc23eb2edb742289ea6d1eea8982600 |
| Source note | uspto-grants-2015_09 |