HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → N,N-Dimethyl-5,5-diphenylpent-4-en-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 5,5-Diphenyl-4-pentenyl bromide | HCID 15550875 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N,N-Dimethyl-5,5-diphenylpent-4-en-1-amine | HCID 20321002 | — |
Reaction Steps
Next, an aqueous solution (40%) of dimethyl amine (25 equivalents) is added slowly to a THF solution of 1.0 equivalent of 5-bromo-1,1-diphenyl-1-pentene that has been obtained in the previous step. The mixture is then stirred at room temperature for 24 hours, and worked up in the usual manner to yield 5-(N,N-dimethyl)amino-1,1-diphenyl-1-pentene as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145352B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-1cc52e4cede243de9d42f18fbaf49008 |
| Source note | uspto-grants-2015_09 |