Urea → HCID 54464597, compound

HRID 2283237Notes

Reaction equation

HRID 2283237 reaction equation
[CH2:1]([C:10]1[CH:15]=[CH:14][C:13]([OH:16])=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].[NH2:17][C:18](N)=[O:19]>>[C:18](=[O:19])([O:16][C:13]1[CH:12]=[CH:11][C:10]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])=[CH:15][CH:14]=1)[NH2:17]

Participants

3

Reactant 2

HCID 1176UreaHCID 17524-Nonylphenol

Product 1

HCID 54464597HCID 54464597, compoundYield 85%

Procedure

The same method as step (6-1) of Example 6 was carried out with the exception of using 11003 g of 4-nonyl phenol (Tokyo Chemical Industry Co., Ltd., Japan) instead of 4-phenyl phenol, using 499 g of urea and carrying out the reaction for 15 hours. When a portion of the reaction liquid was removed and analyzed by liquid chromatography, the formation of (4-nonylphenyl) carbamate was confirmed. The yield was about 85% based on the charged amount of urea.

Workup

  1. customthe reaction for 15 hours
  2. customWhen a portion of the reaction liquid
  3. customwas removed

Sources & evidence

ORD record
ord-48d71748dfbe4ca692623058e4acd180
Source dataset
uspto-grants-2015_09
Patent number
US09145357B2

Reaction notes

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