Urea → HCID 67178891, compound

HRID 2283239Notes

Reaction equation

HRID 2283239 reaction equation
[CH2:1]([C:8]1[CH:13]=[CH:12][C:11]([OH:14])=[CH:10][CH:9]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[NH2:15][C:16](N)=[O:17]>>[C:16](=[O:17])([O:14][C:11]1[CH:10]=[CH:9][C:8]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7])=[CH:13][CH:12]=1)[NH2:15]

Participants

3

Reactant 2

HCID 1176UreaHCID 161434-Heptylphenol

Product 1

HCID 67178891HCID 67178891, compoundYield 90%

Procedure

The same method as step (6-1) of Example 6 was carried out with the exception of using 8040 g of p-heptyl phenol instead of 4-phenyl phenol, using 378 g of urea and carrying out the reaction for 16 hours. When a portion of the reaction liquid was removed and analyzed by liquid chromatography, the formation of (p-pentylphenyl) carbamate was confirmed. The yield was about 90% based on the charged amount of urea.

Workup

  1. customthe reaction for 16 hours
  2. customWhen a portion of the reaction liquid
  3. customwas removed

Sources & evidence

ORD record
ord-1be21657daa04faba526f38c2293c8ed
Source dataset
uspto-grants-2015_09
Patent number
US09145357B2

Reaction notes

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