HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 43532198, compound → HCID 42646992, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 43532198 | HCID 43532198 | — |
| Reactant | 2-AMino-6-fluorobenzenesulfonaMide | HCID 45792644 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 42646992 | HCID 42646992 | 19.2% |
Reaction Steps
2-Amino-6-fluoro-benzenesulfonamide (38 mg, 200 μmol) and (E)-2-(4-phenylphenyl)ethenesulfonyl chloride (56 mg, 200 μmol) were dissolved in pyridine (1.5 mL) and the reaction mixture was shaken for 12 h. The solvent was removed in vacuum and the residues were purified by HPLC to give the product (16.6 mg, 19%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145380B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-e8cd8a2e4883498cbe6466480cee763b |
| Source note | uspto-grants-2015_09 |