HCID 42644132, compound → HCID 42644368, compound

Participants

Reaction Steps

2-[[(E)-2-(4-Chlorophenyl)ethenyl]sulfonylamino]-4-fluoro-benzenesulfonamide (120 mg, 0.31 mmol) was dissolved in ethyl acetate (5 ml) and subjected to the H-cube (1 ml/min, full hydrogen. 10% Pd/C). The product obtained was purified by preparative HPLC (XTerra MS C8 column, acetonitrile/ammonium acetate buffer) to give the title compound (60 mg, 49%) as a white solid.

Provenance & Evidence