HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminobenzenesulfonamide → HCID 57751043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminobenzenesulfonamide | HCID 72894 | — |
| Reactant | 3-Chloro-2-fluorobenzenesulfonyl Chloride | HCID 2778321 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 57751043 | HCID 57751043 | 19.6% |
Reaction Steps
2-Aminobenzenesulfonamide (54 mg, 0.31 mmol) and 3-chloro-2-fluoro-benzenesulfonyl chloride (47 mg, 0.21 mmol) were dissolved in pyridine (1 ml) and the reaction mixture was stirred for 12 h. The solvent was removed in vacuo and the residue was purified by HPLC to give the product (15 mg, 19%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145380B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-cf6a9bc99715492e95210d879f244b70 |
| Source note | uspto-grants-2015_09 |