2-Aminobenzenesulfonamide → HCID 68782416, compound

Participants

Reaction Steps

8-(Methylsulfamoyl)dibenzo[b,d]thiophene-2-sulfonyl chloride (200 mg) was added to a solution of 2-aminobenzenesulfonamide (191 mg) in sulfolane (2 ml). The mixture was stirred at RT for 20 h then diluted with 1N hydrochloric acid. The solid was recovered, washed with 1N hydrochloric acid and dried to give the title compound (196 mg, 72%).

Provenance & Evidence