HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-cyanobenzene-1-sulfonamide → (E)-2-(2-(4-Chloro-2-methoxyphenyl)vinylsulfonamido)-5-cyanobenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-cyanobenzene-1-sulfonamide | HCID 22323994 | — |
| Reactant | 2-(4-Chloro-2-methoxyphenyl)-ethenesulfonyl chloride | HCID 73993005 | — |
| Product | (E)-2-(2-(4-Chloro-2-methoxyphenyl)vinylsulfonamido)-5-cyanobenzenesulfonamide | HCID 57750921 | 27% |
Reaction Steps
The title compound was synthesized as described for Example 178 in 27% yield, starting from 2-amino-5-cyanobenzenesulfonamide and 2-(4-chloro-2-methoxy-phenyl)-ethenesulfonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145380B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-1d4cb220e6534dcd81749710e6e1676d |
| Source note | uspto-grants-2015_09 |