HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Dimethyl-1-butyne → HCID 57751060, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Dimethyl-1-butyne | HCID 13512 | — |
| Reactant | HCID 57750959 | HCID 57750959 | — |
| Product | HCID 57751060 | HCID 57751060 | 34% |
Reaction Steps
The title compound was synthesized as described for Example 179 a) in 34% yield, starting from 2-(2-(6-bromopyridin-3-yl)ethylsulfonamido)benzenesulfonamide and 3,3-dimethyl-1-butyne. Purification by column chromatography, using 10 to 60% ethyl acetate in heptane as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145380B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-4b608d48ac31428fb5b5584fb80a5242 |
| Source note | uspto-grants-2015_09 |