HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminobenzenesulfonamide → HCID 57750970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminobenzenesulfonamide | HCID 72894 | — |
| Reactant | HCID 57751050 | HCID 57751050 | — |
| Product | HCID 57750970 | HCID 57750970 | 69% |
Reaction Steps
The title compound was synthesized as described for Example 178 in 69% yield, starting from 2-aminobenzenesulfonamide and (E)-2-(6-bromopyridin-3-yl)ethenesulfonyl chloride. Purification by column chromatography, using ammonium hydroxide/methanol/chloroform (1:10:89) as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145380B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-0959ecb9c375459ebf59189c034fc80e |
| Source note | uspto-grants-2015_09 |