HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethynylcyclohexane → HCID 57751015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethynylcyclohexane | HCID 70263 | — |
| Reactant | HCID 57750959 | HCID 57750959 | — |
| Product | HCID 57751015 | HCID 57751015 | 25% |
Reaction Steps
The title compound was synthesized as described for Example 179 a) in 25% yield, starting from 2-(2-(6-bromopyridin-3-yl)ethylsulfonamido)benzenesulfonamide and cyclohexylacetylene. Purification by column chromatography using a gradient of 10-60% ethyl acetate in heptane as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145380B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-11aec5bca703445b94b4ce0450f4bc29 |
| Source note | uspto-grants-2015_09 |