huagongshe.com
HRID2283330

反应详情

EQUATION

反应方程式

HRID 2283330 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(N)c(S(N)(=O)=O)c1
HCID245584

2-amino-5-methylbenzenesulfonamide

C7H10N2O2S

结构：O=S(=O)(Cl)/C=C/c1ccc(Br)cc1
HCID23084300

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(NS(=O)(=O)/C=C/c2ccc(Br)cc2)c(S(N)(=O)=O)c1
HCID42644608

未命名化合物

收率 96%

PROCEDURE

实验过程

The title compound was synthesized as described for Example 178 in 96% yield, starting from 2-amino-5-methylbenzenesulfonamide and (E)-2-(4-bromophenyl)ethenesulfonyl chloride (US20040186134 A1). Purification by column chromatography using a gradient of 10-50% ethyl acetate in heptane as the eluent.

WORKUP

后处理

  1. customPurification by column chromatography