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HRID2283340

反应详情

EQUATION

反应方程式

HRID 2283340 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(N)(=O)=O)c(N)c1
HCID11436538

2-amino-4-methylbenzenesulfonamide

C7H10N2O2S

结构：COc1cc(Cl)ccc1/C=C/S(=O)(=O)Cl
HCID22711054

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(Cl)ccc1/C=C/S(=O)(=O)Nc1cc(C)ccc1S(N)(=O)=O
HCID57750912

未命名化合物

收率 69%

PROCEDURE

实验过程

The title compound was synthesized as described for Example 194 a) in 69% yield, starting from 2-amino-4-methylbenzenesulfonamide and (E)-2-(4-chloro-2-methoxyphenyl)ethenesulfonyl chloride (1.5 equiv.). Purification by column chromatography, using chloroform/methanol (95:5) as the eluent.

WORKUP

后处理

  1. customPurification by column chromatography