HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-methylbenzenesulfonamide → 2-[2-(4-Chloro-2-methoxy-phenyl)-ethenesulfonylamino]-5-methyl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-methylbenzenesulfonamide | HCID 245584 | — |
| Reactant | (E)-2-(4-chloro-2-methoxyphenyl)ethenesulfonyl chloride | HCID 22711054 | — |
| Product | 2-[2-(4-Chloro-2-methoxy-phenyl)-ethenesulfonylamino]-5-methyl-benzenesulfonamide | HCID 68782634 | 81% |
Reaction Steps
The title compound was synthesized as described for Example 194 a) in 81% yield, starting from 2-amino-5-methylbenzenesulfonamide and (E)-2-(4-chloro-2-methoxyphenyl)ethenesulfonyl chloride (1 equiv.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145380B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-d358716c455d49b8b3a1a7553e065d93 |
| Source note | uspto-grants-2015_09 |