HRID2283356

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID13512

3,3-Dimethylbutyne

C6H10

结构：NS(=O)(=O)c1cc(CO)ccc1NS(=O)(=O)CCc1ccc(Br)cc1

HCID57751051

未命名化合物

PRODUCTS

生成物

结构：CC(C)(C)C#Cc1ccc(CCS(=O)(=O)Nc2ccc(CO)cc2S(N)(=O)=O)cc1

HCID57751100

未命名化合物

收率 5%

PROCEDURE

实验过程

The title compound was synthesized as described for Example 210 in 5% yield, starting from 2-[2-(4-bromo-phenyl)-ethanesulfonylamino]-5-hydroxymethyl-benzenesulfonamide and 3,3-dimethyl-1-butyne. Purification by preparative HPLC.

WORKUP

后处理

customPurification by preparative HPLC