HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Dimethyl-1-butyne → HCID 57750930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Dimethyl-1-butyne | HCID 13512 | — |
| Reactant | HCID 57750944 | HCID 57750944 | — |
| Product | HCID 57750930 | HCID 57750930 | 18% |
Reaction Steps
The title compound was synthesized as described for Example 210 in 18% yield, starting from 3-[2-(4-bromo-phenyl)-ethanesulfonylamino]-thiophene-2-sulfonic acid amide and 3,3-dimethyl-1-butyne. Purification by column chromatography, using 50% ethyl acetate in hexanes as the eluent, followed by purification by preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145380B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-78ee4dfebcb048c18efe9b00a43af496 |
| Source note | uspto-grants-2015_09 |