HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-4-(trifluoromethyl)benzene → HCID 59635822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-4-(trifluoromethyl)benzene | HCID 4348295 | — |
| Reactant | HCID 57750959 | HCID 57750959 | — |
| Product | HCID 59635822 | HCID 59635822 | 28% |
Reaction Steps
The title compound was synthesized as described for Example 179 a) in 28% yield, starting from 2-(2-(6-bromopyridin-3-yl)ethylsulfonamido)benzenesulfonamide and 4-ethynyl-alpha,alpha,alpha-trifluorotoluene. Purification by preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145380B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-252fb401c41744418f31fe3d7bab0043 |
| Source note | uspto-grants-2015_09 |