HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22316709, compound → 4-(Methanesulfonyl)-2-methoxyaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22316709 | HCID 22316709 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(Methanesulfonyl)-2-methoxyaniline | HCID 22316785 | 98.1% |
Reaction Steps
A suspension of 2-methoxy-4-(methylsulfonyl)-1-nitrobenzene (0.175 g, 0.76 mmol) and palladium on carbon (10 wt %, 0.10 g) in ethanol (10 mL) was stirred under hydrogen at one atmosphere pressure for 18 hours. The reaction was filtered through celite and concentrated to give 2-methoxy-4-(methylsulfonyl)aniline (0.15 g, 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145402B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-d37c5a4e6ec54e1290828c6f846fdbcb |
| Source note | uspto-grants-2015_09 |