Iodoethane → HCID 69671261, compound
Reaction equation
[N+:1]([C:4]1[CH:12]=[CH:11][CH:10]=[C:9]2[C:5]=1[CH:6]=[N:7][NH:8]2)([O-])=O.I[CH2:14][CH3:15]>>[CH2:14]([N:7]1[CH:6]=[C:5]2[C:9]([CH:10]=[CH:11][CH:12]=[C:4]2[NH2:1])=[N:8]1)[CH3:15]Participants
3
Procedure
In accordance with Example 4 (Steps 1 and 2), 4-nitro-1H-indazole was used instead of 5-nitro-1H-indazole, and 2-iodoethane was used instead of ethyl bromide-d5 to obtain 2-ethyl-2H-indazol-4-amine.
Sources & evidence
- ORD record
- ord-9bc160acabd14beeacbc3c4779464c19
- Source dataset
- uspto-grants-2015_09
- Patent number
- US09145414B2
Reaction notes
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