HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90308781, compound → HCID 90308716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90308781 | HCID 90308781 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 90308716 | HCID 90308716 | — |
Reaction Steps
10% Palladium on carbon (1.0 g) was added to a solution of 1-ethyl-4-methyl-6-nitro-1H-indazole obtained in the above-described Step 1 (975 mg) in ethyl acetate (10 mL), and the reaction solution was stirred under hydrogen atmosphere at room temperature overnight. The insolubles were filtrated, and the solvent was evaporated under vacuum to obtain 1-ethyl-4-methyl-1H-indazol-6-amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145414B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-65501ae3b5474f9587f9b02a27634654 |
| Source note | uspto-grants-2015_09 |