Iodoethane → HCID 90308748, compound

HRID 2283713Notes

Reaction equation

HRID 2283713 reaction equation
[Br:1][C:2]1[CH:10]=[C:9]([C:11]([O:13][CH3:14])=[O:12])[CH:8]=[C:7]2[C:3]=1[CH:4]=[N:5][NH:6]2.I[CH2:16][CH3:17]>>[Br:1][C:2]1[CH:10]=[C:9]([C:11]([O:13][CH3:14])=[O:12])[CH:8]=[C:7]2[C:3]=1[CH:4]=[N:5][N:6]2[CH2:16][CH3:17]

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 24728060Methyl 4-bromo-1H-indazole-6-carboxylate

Product 1

HCID 90308748HCID 90308748, compound

Procedure

In accordance with Example 4 (Steps 1 and 2), methyl 4-bromo-1H-indazole-6-carboxylate was used instead of 5-nitro-1H-indazole, and 2-iodoethane was used instead of ethyl bromide-d5 to obtain methyl 4-bromo-1-ethyl-1H-indazole-6-carboxylate.

Sources & evidence

ORD record
ord-e829741480f448b3aa75f2eaff23797e
Source dataset
uspto-grants-2015_09
Patent number
US09145414B2

Reaction notes

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