HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66958288, compound → HCID 66959005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66958288 | HCID 66958288 | — |
| Solvent | Phosphorus oxychloride | HCID 24813 | — |
| Product | HCID 66959005 | HCID 66959005 | 98.7% |
Reaction Steps
5-Ethyl-1-propyl-1H-pyrazole-3-carboxamide (5.50 g, 30.35 mmol) was treated with phosphorous oxychloride (20 mL) according to the procedure described in Part D of Examples 37-39 to yield 4.89 g of 5-ethyl-1-propyl-1H-pyrazole-3-carbonitrile as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145410B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-92b5d0bda313494f8a4cfbc4971e1e2a |
| Source note | uspto-grants-2015_09 |