HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2284101Generated: October 30, 2026
Trifluoroacetic acid → HCID 22692035, compound
https://huagongshe.com/reaction/2284101
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Carbamic acid, N-[3-[[2-(3-methoxyphenyl)ethyl]amino]-3-oxopropyl]-, 1,1-dimethylethyl ester | HCID 86673951 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22692035 | HCID 22692035 | — |
Reaction Steps
tert-butyl (3-((3-methoxyphenethyl)amino)-3-oxopropyl)carbamate was dissolved in dichloromethane (0.5 mL) then the solution was cooled to 0° C. in an ice bath. Trifluoroacetic acid (300 μL) was added then the solution was allowed to warm slowly to room temperature with stirring. Upon completion of the reaction the solvent is removed under reduced pressure to give crude product which is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09144557B2 |
|---|
| Source dataset | uspto-grants-2015_09 |
|---|
| ORD ID | ord-0f079fbe990847d9b8c77bbaddc2d28a |
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| Source note | uspto-grants-2015_09 |
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