4-Methoxybenzaldehyde → HCID 178488860, compound

HRID 2284125Notes

Reaction equation

[N+:1]([C:4]1[CH:5]=[C:6]([CH:15]=[CH:16][C:17]=1[N+:18]([O-])=O)[NH:7][C:8]([C:10]1[S:11][CH:12]=[CH:13][CH:14]=1)=[O:9])([O-])=O.[CH3:21][O:22][C:23]1[CH:30]=[CH:29][C:26]([CH:27]=O)=[CH:25][CH:24]=1>>[CH3:21][O:22][C:23]1[CH:30]=[CH:29][C:26]([C:27]2[NH:18][C:17]3[CH:16]=[CH:15][C:6]([NH:7][C:8]([C:10]4[S:11][CH:12]=[CH:13][CH:14]=4)=[O:9])=[CH:5][C:4]=3[N:1]=2)=[CH:25][CH:24]=1

Participants

Reactant 2

HCID 312444-Methoxybenzaldehyde

HCID 86673965HCID 86673965, compound

Product 1

HCID 178488860HCID 178488860, compound

Procedure

Compound 210 was prepared according to the procedure similar to that described in Scheme III from 3,4-dinitro-N-(thien-2-oyl)aniline and 4-methoxybenzaldehyde. [M+H]+ calcd for C19H15N3O2S: 350.09; found: 349.89.

Sources & evidence

ORD record: ord-ed41e2fb74f042aaa84182210af68d31
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09144557B2

Reaction notes

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