P-Phenylenediamine → HCID 136441224, compound

HRID 2284168Notes

Reaction equation

[N:1]1([C:7]2[CH:12]=[CH:11][C:10]([C:13]3[NH:14][C:15]4[CH:21]=[C:20]([C:22]([OH:24])=O)[CH:19]=[CH:18][C:16]=4[N:17]=3)=[CH:9][CH:8]=2)[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[C:25]1([NH2:32])[CH:30]=[CH:29][C:28]([NH2:31])=[CH:27][CH:26]=1>>[C:25]1([NH:32][C:22]([C:20]2[CH:19]=[CH:18][C:16]3[NH:17][C:13]([C:10]4[CH:9]=[CH:8][C:7]([N:1]5[CH2:6][CH2:5][O:4][CH2:3][CH2:2]5)=[CH:12][CH:11]=4)=[N:14][C:15]=3[CH:21]=2)=[O:24])[CH:30]=[CH:29][C:28]([NH:31][C:22]([C:20]2[CH:19]=[CH:18][C:16]3[NH:17][C:13]([C:10]4[CH:9]=[CH:8][C:7]([N:1]5[CH2:2][CH2:3][O:4][CH2:5][CH2:6]5)=[CH:12][CH:11]=4)=[N:14][C:15]=3[CH:21]=2)=[O:24])=[CH:27][CH:26]=1

Participants

Reactant 2

HCID 7814P-Phenylenediamine

HCID 67112227HCID 67112227, compound

Product 1

HCID 136441224HCID 136441224, compound

Procedure

Compound 280 was prepared according to the procedure similar to that described in Scheme V from 2-(4-morpholinylphenyl)benzimidazole-5-carboxylic acid and 1,4-phenylenediamine. [M+H]+ calcd for C42H38N8O4: 719.30; found: 719.12.

Sources & evidence

ORD record: ord-b9896dc30e884435bdbd04db30297ccc
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09144557B2

Reaction notes

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