HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-cyclopropoxyethanol → HCID 66726625, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-cyclopropoxyethanol | HCID 12023383 | — |
| Reactant | 2,5,6-Trichloropyridine-3-carboxamide | HCID 53750930 | — |
| Reactant | 1,3-Dihydro-1-hydroxy-2,1-benzoxaborol-5-ol | HCID 57968699 | — |
| Product | HCID 66726625 | HCID 66726625 | — |
Reaction Steps
This compound was prepared from 2,5,6-trichloronicotinamide, 2-cyclopropoxyethanol, and benzo[c][1,2]oxaborole-1,5(3H)-diol in a similar manner to that of D230. 1H-NMR (400 MHz, DMSO-d6) δ (ppm) 0.35-0.4 (m, 4H), 3.2-3.32 (m, 1H), 3.55-3.62 (m, 3H), 4.1-4.12 (m, 2H), 5.0 (s, 2H), 7.24 (dd, J=6.0, 1.4 Hz, 1H), 7.33 (s, 1H), 7.8 (d, J=6.7 Hz, 1H), 8.6 (s, 1H), 9.26 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145429B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-72593f2bd6724e6a9b71d40f3c241e06 |
| Source note | uspto-grants-2015_09 |