HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 178449832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Sodium Sulfate | HCID 24436 | — |
| Reactant | tert-butyl N-(2-amino-2-methylpropyl)carbamate | HCID 17909918 | — |
| Solvent | Benzaldehyde | HCID 240 | — |
| Product | HCID 178449832 | HCID 178449832 | — |
Reaction Steps
To a suspension of tert-butyl (2-amino-2-methylpropyl)carbamate (1.98 g) and anhydrous sodium sulfate (3.00 g) in toluene (5 mL), benzaldehyde (1.07 mL) was added at room temperature, and the mixture was stirred for 11 hours under reflux by heating. The reaction mixture was cooled to room temperature, and then the solvent was evaporated under reduced pressure to obtain (E)-tert-butyl (2-(benzylideneamino)-2-methylpropyl)carbamate (G8).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145415B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-0db8ab7d317b42abb605884a8f0e2d1d |
| Source note | uspto-grants-2015_09 |