Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl ethylphosphonate → Aluminum ethyl ethylphosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl ethylphosphonate | HCID 6534 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Aluminum sulfate (USP) | HCID 3080712 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Aluminum ethyl ethylphosphonate | HCID 86673924 | 100.7% |
반응 단계
Aluminum ethyl ethylphosphonate was prepared according to a known procedure: Diethyl ethylphosphonate (414 g), sodium hydroxide (199.5), and water (2.4 L) were refluxed for 4 h. A solution of aluminum sulfate hydrate (261 g) in water (830 mL) was then slowly added to form a white slurry. After filtration and drying, 319.7 g of aluminum ethyl ethylphosphonate was obtained as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09145488B2 |
| 출처 데이터셋 | uspto-grants-2015_09 |
| ORD ID | ord-ff985fbea80d48cabf5dfe46619968ce |
| 출처 메모 | uspto-grants-2015_09 |