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HRID2284825

反应详情

EQUATION

反应方程式

HRID 2284825 的结构方程式

REACTANTS

反应物

3
结构：CCOP(=O)(CC)OCC
HCID6534

Diethyl ethylphosphonate

C6H15O3P

结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：O.O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].[Al+3].[Al+3]
HCID3080712

未命名化合物

PRODUCTS

生成物

1
结构：CCOP(=O)([O-])CC.CCOP(=O)([O-])CC.CCOP(=O)([O-])CC.[Al+3]
HCID86673924

未命名化合物

收率 100.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

2 次

PROCEDURE

实验过程

Aluminum ethyl ethylphosphonate was prepared according to a known procedure: Diethyl ethylphosphonate (414 g), sodium hydroxide (199.5), and water (2.4 L) were refluxed for 4 h. A solution of aluminum sulfate hydrate (261 g) in water (830 mL) was then slowly added to form a white slurry. After filtration and drying, 319.7 g of aluminum ethyl ethylphosphonate was obtained as a white solid.

WORKUP

后处理

  1. customAluminum ethyl ethylphosphonate was prepared
  2. customto form a white slurry
  3. filtrationAfter filtration
  4. customdrying