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HRID2284826

反应详情

EQUATION

反应方程式

HRID 2284826 的结构方程式

REACTANTS

反应物

3
结构：CCOP(=O)(OCC)OCC
HCID6535

Triethyl phosphate

C6H15O4P

结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：O.O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].[Al+3].[Al+3]
HCID3080712

未命名化合物

PRODUCTS

生成物

1
结构：CCOP(=O)([O-])[O-].CCOP(=O)([O-])[O-].CCOP(=O)([O-])[O-].[Al+3].[Al+3]
HCID86673925

未命名化合物

收率 260.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

2 次

PROCEDURE

实验过程

Aluminum ethylphosphate was prepared according to a known procedure: Triethylphosphate (40 g), sodium hydroxide (17.5 g), and water (0.4 L) were refluxed for 2.5 h. A solution of aluminum sulfate hydrate (23.8 g) in water (300 mL) was then slowly added to form a white slurry. After filtration and drying, 36.7 g of aluminum ethylphosphate was obtained as a white solid.

WORKUP

后处理

  1. customAluminum ethylphosphate was prepared
  2. customto form a white slurry
  3. filtrationAfter filtration
  4. customdrying