HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl 3-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)benzoate → 3-[3-tert-Butyl-5-(2,2,2-trichloro-ethoxycarbonylamino)-pyrazol-1-yl]-benzoic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl 3-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)benzoate | HCID 21867322 | — |
| Reactant | [5-tert-Butyl-2-(3-hydroxymethyl-phenyl)-2H-pyrazol-3-yl]-carbamic acid 2,2,2-trichloro-ethyl ester | HCID 86687007 | — |
| Product | 3-[3-tert-Butyl-5-(2,2,2-trichloro-ethoxycarbonylamino)-pyrazol-1-yl]-benzoic acid ethyl ester | HCID 86687008 | — |
Reaction Steps
The title compound was prepared from Intermediate 29a using an analogous procedure to that described for Intermediate 29c. LCMS (Method 3): Rt 4.67 min, m/z 462, 464 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145413B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-847169bcdaf340ebbe7e5916f9a5f7fc |
| Source note | uspto-grants-2015_09 |