HRID228511

反应详情

EQUATION

反应方程式

HRID 228511 的结构方程式

PROCEDURE

实验过程

4-(2,4-Dimethylphenoxy)-6,7-dimethoxyquinoline (99 mg) was dissolved in a 10% hydrochloric acid/methanol solution, and the solution was stirred at room temperature for 15 min. The solvent was removed therefrom by distillation under the reduced pressure, and the residue was washed with ethyl acetate to give the title compound (94 mg, yield 85%).

WORKUP

后处理

  1. customThe solvent was removed
  2. distillationby distillation under the reduced pressure
  3. washthe residue was washed with ethyl acetate