HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 23078607, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | 4-(2,4-Dimethylphenoxy)-6,7-dimethoxyquinoline | HCID 23078253 | — |
| Product | HCID 23078607 | HCID 23078607 | 85% |
Reaction Steps
4-(2,4-Dimethylphenoxy)-6,7-dimethoxyquinoline (99 mg) was dissolved in a 10% hydrochloric acid/methanol solution, and the solution was stirred at room temperature for 15 min. The solvent was removed therefrom by distillation under the reduced pressure, and the residue was washed with ethyl acetate to give the title compound (94 mg, yield 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560558B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-f137a51d6c564a2f84dddce0cd7ba159 |
| Source note | uspto-grants-2009_07 |