HRID228524

反应详情

EQUATION

反应方程式

HRID 228524 的结构方程式

PROCEDURE

实验过程

6,7-Dimethoxy-4-(3,4-dimethylphenoxy)quinoline (122 mg) was dissolved in a 10% hydrochloric acid/methanol solution, and the solution was stirred at room temperature for 15 min. The solvent was removed therefrom by distillation under the reduced pressure. The residue was washed with ethyl acetate to give the title compound (118 mg, yield 87%).

WORKUP

后处理

  1. customThe solvent was removed
  2. distillationby distillation under the reduced pressure
  3. washThe residue was washed with ethyl acetate