HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → 6,7-Dimethoxy-4-(3,4-dimethylphenoxy)quinoline hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | 6,7-Dimethoxy-4-(3,4-dimethylphenoxy)quinoline | HCID 23078387 | — |
| Product | 6,7-Dimethoxy-4-(3,4-dimethylphenoxy)quinoline hydrochloride | HCID 23078545 | 87% |
Reaction Steps
6,7-Dimethoxy-4-(3,4-dimethylphenoxy)quinoline (122 mg) was dissolved in a 10% hydrochloric acid/methanol solution, and the solution was stirred at room temperature for 15 min. The solvent was removed therefrom by distillation under the reduced pressure. The residue was washed with ethyl acetate to give the title compound (118 mg, yield 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560558B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-d4b6650a7ad546d89649f5741e9d45db |
| Source note | uspto-grants-2009_07 |