HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butanethiol → HCID 20544206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butanethiol | HCID 8012 | — |
| Reactant | 4-Nitro-2-trichloromethylbenzenesulfenyl chloride | HCID 12763555 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20544206 | HCID 20544206 | 92.1% |
Reaction Steps
61 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride in 800 ml of diethyl ether is reacted in a stirred apparatus with 18 g of 1-butylmercaptan for 6 hours at 25° C. The completion of the reaction is determined by gas chromatography. After removal of the solvent, there is obtained 66 g (92% of theory) of (4-nitro-2-trichloromethylphenyl)-n-butyl disulfide as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04324793 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-cf198ab545684497b81619fb8349f1d8 |
| Source note | uspto-grants-1982_04 |