HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Dodecanethiol → (4-Nitro-2-trichloromethylphenyl)-dodecyl disulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Dodecanethiol | HCID 8195 | — |
| Reactant | 4-Nitro-2-trichloromethylbenzenesulfenyl chloride | HCID 12763555 | — |
| Product | (4-Nitro-2-trichloromethylphenyl)-dodecyl disulfide | HCID 20544208 | 86% |
Reaction Steps
As in Example 1, 61.4 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride is reacted with 40.5 g of dodecyl-mercaptan. There is obtained 81 g (86% of theory) of (4-nitro-2-trichloromethylphenyl)-dodecyl disulfide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04324793 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-a39b9df5010d4ca3af6f3256f5778dfd |
| Source note | uspto-grants-1982_04 |