HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioglycolic Acid → HCID 20544199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | 4-Nitro-2-trichloromethylbenzenesulfenyl chloride | HCID 12763555 | — |
| Product | HCID 20544199 | HCID 20544199 | 85.6% |
Reaction Steps
As in Example 1, 61.4 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride is reacted with 18.4 g of thioglycolic acid. After the solvent has been distilled off and the residue recrystallized from toluene, there is obtained 62 g of carboxymethyldithio-4-nitro-2-trichloromethylbenzene; m.p.: 140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04324793 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-8ff28fb007b546f3ab681f64afb4f3e8 |
| Source note | uspto-grants-1982_04 |