HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 12932087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(5-chloro-2-methoxyphenyl)propan-1-ol | HCID 266745 | — |
| Product | HCID 12932087 | HCID 12932087 | — |
Reaction Steps
58.2 g of 3-(5-chloro-2-methoxyphenyl)propan-1-ol and 50 ml of thionyl chloride are stirred at 50° for 8 hours; the excess thionyl chloride is distilled off in vacuo and the residue is distilled under a high vacuum. 50.9 g of 3-(5-chloro-2-methoxyphenyl)propyl chloride of b.p. 87° to 95° under 0.005 mm Hg are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04324796 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-1e7a2a9b6b184db8ae0b8e151812eaa5 |
| Source note | uspto-grants-1982_04 |