Calcium Chloride → HCID 86738335, compound

HRID 2285759Notes

Reaction equation

HRID 2285759 reaction equation
[Cl-].[Ca+2:2].[Cl-].[C:4]1([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:15]2([C:18]([O-:20])=[O:19])[CH2:17][O:16]2)[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[Na+]>O>[Ca:2].[C:4]1([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:15]2([C:18]([O-:20])=[O:19])[CH2:17][O:16]2)[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=1

Participants

4

Reactant 2

HCID 5284359Calcium ChlorideHCID 23676476Sodium 2-(5-phenylpentyl)oxirane-2-carboxylate

Product 1

HCID 86738335HCID 86738335, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A solution of 400 mg calcium chloride in 5 ml of water is added dropwise to a solution of 1.0 g of sodium 2-(5-phenylpentyl)oxirane-2-carboxylate in 30 ml of water. The mixture is stirred thoroughly. The solution is decanted from the viscous precipitate which has separated out. The precipitate is stirred again with water and decanted. After drying over phosphorus pentoxide 820 mg of the title compound (softening at 270° C. and melting at about 300° C. under decomposition) are obtained.

Workup

  1. customThe solution is decanted from the viscous precipitate which
  2. customhas separated out
  3. stirringThe precipitate is stirred again with water
  4. customdecanted
  5. dry with materialAfter drying over phosphorus pentoxide 820 mg of the title compound (softening at 270° C. and melting at about 300° C. under decomposition)
  6. customare obtained

Sources & evidence

ORD record
ord-151c835eb22c44debd0be2bbf3f28fa1
Source dataset
uspto-grants-1982_04
Patent number
US04324796

Reaction notes

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