Hydrochloric Acid → HCID 15571273, compound

HRID 2285897Notes

Reaction equation

HRID 2285897 reaction equation
[C:1]1([CH:7]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[C:8]2([OH:18])[N:12]3[CH2:13][CH2:14][CH2:15][CH2:16][N:17]=[C:11]3[S:10][CH2:9]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:25]>CC(C)=O>[ClH:25].[C:19]1([CH:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:8]2([OH:18])[N:12]3[CH2:13][CH2:14][CH2:15][CH2:16][N:17]=[C:11]3[S:10][CH2:9]2)[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 15571271HCID 15571271, compound

Product 1

HCID 15571273HCID 15571273, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A solution of 3.0 g. of 3-diphenylmethyl-2,3,5,6,7,8-hexahydrothiazolo[3,2-a][1,3]diazepin-3-ol in 30 ml. of acetone is treated with 4 ml. of 3 N ethanolic hydrochloric acid. The resulting solid is collected by filtration, giving the desired product, m.p. 205° C. (dec.).

Workup

  1. filtrationThe resulting solid is collected by filtration

Sources & evidence

ORD record
ord-ac8147fed8a54ebdbddaff8297f2f24d
Source dataset
uspto-grants-1982_04
Patent number
US04325955

Reaction notes

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