HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → p-Chlorobenzylmercaptoacetohydroxamic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | Methyl 2-(4-chlorobenzylthio)acetate | HCID 3311340 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | p-Chlorobenzylmercaptoacetohydroxamic acid | HCID 54399917 | — |
Reaction Steps
A solution of 0.15 mol of methyl 2-(4-chlorobenzylmercapto)-acetate in 50 ml of methanol is mixed with a solution of 0.225 mol of hydroxylamine (base) and 0.15 mol of NaOH3 in 150 ml of methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04325964 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-81d2853274df44a99243bae0279f314f |
| Source note | uspto-grants-1982_04 |